Course title
M20650001
Instrumental Analysis

 PAOLO MELE

SAKAI Naomichi

RZEZNICKA IZABELA IRENA

AHMED KUMKUM
and more...

LEE SO YOON

KLIMKOWICZ ALICJA
Course description
The theoretical classes (1, 3, 5, 8, 10, 12) and exam classes (7 and 14) are held virtually, but the laboratory classes (2, 4, 6, 9, 11, 13) are held in person.
In order to become an excellent engineer or researcher, it is mandatory to afford experiments in laboratory and know the theory behind experimental techniques. This course is given by international faculty members. Various experimental techniques are introduced such as: X-Ray Diffraction (XRD); Physical Properties Measurement System (PPMS); Scanning Electron Microscopy (SEM; Thermogravimetry and Differential Thermal Analysis (TG/DTA); Fourier-Transform Infra-Red spectroscopy (FT-IR); Raman spectroscopy. For each technique, one class about working principles and introduction to the chemical and/or physical theory behind will be given, followed by a class of basic experience in laboratory. The students will be divided in small groups (3 or 4 each) and each group will team to prepare the reports and presentations of each experience.
Purpose of class
The students will be able to use the standard characterization techniques which constitute the grounds of applied materials science. Students will be able to explain the basic scientific and technical principles of advanced equipment and apply them in the laboratory, to obtain reliable data.They will also obtain experience on how to work in a team, write experimental reports and prepare presentations.
Goals and objectives

 Goals and objectives Course Outcomes
1. Students will be able to explain the basic scientific and technical principles of several measuring techniques used in material science.
A-1
2. Students will be able to explain the theoretical principles of the instruments and conduct basic experiments in the lab.
A-1
3. The students will be able to write scientific reports .
A-1
4. The students will be able to prepare and deliver public presentations.
A-1
Language
English
Class schedule

 Class schedule HW assignments (Including preparation and review of the class.) Amount of Time Required
1. Introduction to the course - explanation on how prepare reports and presentations;
XRD - theory and principles 		lecture review at home 170分
2. XRD - laboratory preparation of report at home 170分
3. PPMS - principles of transport measurements lecture review at home 170分
4. PPMS -laboratory preparation of report at home 170分
5. Electron microscopies and SEM - laboratory lecture review at home 170分
6. Electron microscopies and SEM - theory preparation of report at home 170分
7. First part: discussion of reports of the first three laboratories (XRD, PPMS, and SEM) and presentation in the class on a technique of choice of the first three preparation for first part (reports and presentation) 305分
8. TG/DTA -theory lecture review at home 170分
9. TG/DTA - laboratory preparation of report at home 170分
10. FT-IR spectroscopy -theory lecture review at home 170分
11. FT-IR spectroscopy - laboratory preparation of report at home 170分
12. Raman specroscopy - theory lecture review at home 170分
13. Raman specroscopy - laboratory preparation of report at home 170分
14. Second part: discussion of reports of the second three laboratories (TG/DTA, FT-IR and Raman spectroscopy) and presentation in the class on a technique of choice of the second three preparation for second part (reports and presentation) 305分
Total. - - 2650分
Relationship between 'Goals and Objectives' and 'Course Outcomes'

 Reports 1, 2, 3 Reports 4, 5, 6 Presentation I Presentation II Total.
1. 30% 30%
2. 30% 30%
3. 20% 20%
4. 20% 20%
Total. 30% 30% 20% 20% -
Evaluation method and criteria
Each report will contribute for 10% to student`s grade.
Totally 6 reports must be provided (for every experimental class) so total score for the reports is at maximum 60% of the grade

Each presentation will contribute for 20% to student`s grade. Totally 2 presentations must be provided (for one technique of choice from the first three and for one technique of choice from the second three) so total score for the presentations is at maximum 40% of the grade

To pass the student must earn a total score of 60% or more.
Textbooks and reference materials
Handouts and manuals distributed in classroom
Prerequisites
Basic Chemistry, Basic Physics
Office hours and How to contact professors for questions
  • Contact via e-mail, the e-mail addresses to the teachers of each class to establish an appointment (substitute "[at] with "@")
  • Introduction and coordination: P. Mele pmele[at]shibaura-it.ac.jp
    XRD: A. Klimkowicz alicja[at]shibaura-it.ac.jp
    PPMS: N. Sakai nsakai[at]shibaura-it.ac.jp
  • SEM: K. Ahmed kumkum[at]shibaura-it.ac.jp
    TG/DTA: K. Ahmed kumkum[at]shibaura-it.ac.jp
  • FT-IR: S. Y. Lee soyoon[at]shibaura-it.ac.jp
    Raman: I. I. Rzeznicka izabela[at]shibaura-it.ac.jp
Regionally-oriented
Non-regionally-oriented course
Development of social and professional independence
  • Course that cultivates an ability for utilizing knowledge
  • Course that cultivates a basic problem-solving skills
Active-learning course
About half of the classes are interactive
Course by professor with work experience
Work experience Work experience and relevance to the course content if applicable
N/A N/A
Education related SDGs:the Sustainable Development Goals
  • 7.AFFORDABLE AND CLEAN ENERGY
  • 9.INDUSTRY, INNOVATION AND INFRASTRUCTURE
  • 12.RESPONSIBLE CONSUMPTION & PRODUCTION
Last modified : Sat May 28 04:05:51 JST 2022