Analytical Chemistry Laboratory

Course title

D0350100

	MASADOME Takashi
	OGUCHI Hiroyuki
	KIYONO Hajime
	YAMASHITA Mitsuo
and more...
	OISHI Tomoji
	KAWANO Yasuro
	KUDOH Satoshi
	NAKAJIMA Hiromitsu

Course description

Students must master the operation of basic chemistry experiment. In addition, students must fully learn the basics of analytical chemistry, such as the calculation of the gravimetric analysis and volumetric analysis by doing the gravimetric and volumetric analysis experiments repeatedly.

Purpose of class

Goals and objectives

Students can master the basic analytical chemistry experiment by considering of safety and environment
Students can master the calculation of the gravimetric and volumetric analysis
Students can submit the well-formatd experiment report

Language

English

Class schedule

Class schedule	HW assignments (Including preparation and review of the class.)	Amount of Time Required
Preparation of experiment	read the text book in detail	200minutes
Acid-base titration (standardization of HCl standard solution, determination of NaOH and Na2CO3, respectively)	read the text book in detail	200minutes
Redox titration（Standardization of KMnO4 standard solution, Determination of Fe in Fe salt using redox titration)	read the text book in detail	200minutes
Determination of SO4（Determination of SO4 in CuSO4 5H2O by gravimetric analysis）	read the text book in detail	200minutes
Determination of Fe in Fe salt by gravimetric analysis	read the text book in detail	200minutes
Determination of Ni (Determination of Ni using dimethylglyoxime as a precipitation reagent)	read the text book in detail	200minutes
chelatometric titration (Determination of metal ion by using EDTA)	read the text book in detail	200minutes
Precipitation titration（Determination of halogen ion using Mohr method and Vorhard method )	read the text book in detail	200minutes
Ion exchange（Separation and determination of metal ions using an ion-exchange resin)	read the text book in detail	200minutes
Lecture (calculations for concentration of solution, titration and gravimetric analysis)	read the text book in detail	200minutes
Exercises １（calculations for concentration of solution, titration and gravimetric analysis）	read the text book in detail	200minutes
Exercises２（calculations for concentration of solution, titration and gravimetric analysis）	read the text book in detail	200minutes
Exercises３（calculations for concentration of solution, titration and gravimetric analysis）	read the text book in detail	200minutes
Exercises４（calculations for concentration of solution, titration and gravimetric analysis）	read the text book in detail	200minutes
-	-	2800minutes

Relationship between 'Goals and Objectives' and 'Course Outcomes'

	Report	Practice	Total.
1.	20%		20%
2.	10%	20%	30%
3.	50%		50%
Total.	80%	20%	-

Evaluation method and criteria

With experiment reports which include the topics of "goals and the objectives"(80%) , test of exercises during classes which include the topics of "goals and the objectives".(20%), for a total possible score of 100, a total score of 60 or above will be required for a passing grade. As well, credits for this course will not be awarded if a student fails to attend more than 1 class.

Textbooks and reference materials

Textbooks are prepared for graduate students.
References:Analytical Chemistry 6th Ed.／G. D. Christian／Wiley, Analytical Chemistry／R. Kellner ed. / Wiley-VCH, Textbooks of analytical chemistry, physical Chemistry and electrochemistry used in an undergraduate course.

Prerequisites

Taking of course of Analytical Chemistry１

Office hours and How to contact professors for questions