Course title
D00190003
Laboratory Course of Organic Chemistry

 KITAGAWA Osamu
Course description
Synthesis of several organic compounds through organic reactions such as Grignard reaction, aldol reaction and hydride reduction，
Structural analysis of organic compounds by 1H-NMR and IR spectroscopy.
Purpose of class
Further understanding on organic reactions and instrument analyses that learned in classes of organic chemistry and structural determination method of organic compounds.
Acquisition of fundamental skill on experimental procedure, instrumental analysis and preparation of experiment report.
Goals and objectives
  1. Preparation of target organic compounds in accordance with experimental procedure
  2. Acquisition of fundamental experimental procedure
  3. Structural determination of target organic compound through instrumental analyses
  4. Preparation of experiment report
  5. Understanding of danger of organic solvents and reagents
Relationship between 'Goals and Objectives' and 'Course Outcomes'

 experiment report Total.
1. 10% 10%
2. 10% 10%
3. 10% 10%
4. 60% 60%
5. 10% 10%
Total. 100% -
Evaluation method and criteria
It will be evaluated by experiment report.
Language
English
Class schedule

 Class schedule HW assignments (Including preparation and review of the class.) Amount of Time Required
1. Lecture on purpose and significance of laboratory course of organic chemistry (First group) Reading of experimental text 190minutes
2. The reaction using Grignard reagent: Synthesis of triphenylmethanol (First group) Reading of experimental text 570minutes
3. Structural determination of triphenylmethanol：mesurement of melting point and IR spectrum (First group) Reading of experimental text 570minutes
4. Aldol condensation of acetone and benzaldehyde (First group) Reading of experimental text 570minutes
5. Reduction of acetophenone by NaBH4: Synthesis of 1-phenylethanol (First group) Reading of experimental text 380minutes
6. 1H-NMR and IR measurement of 1-phenylethanol and its structural analysis (First group) Reading of experimental text 570minutes
7. The reaction using Grignard reagent: Synthesis of triphenylmethanol (Second group) Reading of experimental text 570minutes
8. Structural determination of triphenylmethanol：mesurement of melting point and IR spectrum (Second group) Reading of experimental text 570minutes
9. Aldol condensation of acetone and benzaldehyde (Second group) Reading of experimental text 570minutes
10. Reduction of acetophenone by NaBH4: Synthesis of 1-phenylethanol (Second group) Reading of experimental text 570minutes
11. 1H-NMR and IR measurement of 1-phenylethanol and its structural analysis (First group) Reading of experimental text 570minutes
12. Preparation of Experimental Report 1 (Grignard reaction) Reading of experimental text 570minutes
13. Preparation of Experimental Report 2 (Aldol reaction) Reading of experimental text 570minutes
14. Preparation of Experimental Report 3 (Hydride reduction) Reading of experimental text 570minutes
Total. - - 7410minutes
Feedback on exams, assignments, etc.
ways of feedback specific contents about "Other"
Feedback in the class
Textbooks and reference materials
Experimental text will be distributed.
Prerequisites
Basic knowledge on organic chemistry will be required.
Office hours and How to contact professors for questions
  • Wednesday 10:00 am - 12:00 am
Regionally-oriented
Non-regionally-oriented course
Development of social and professional independence
  • Course that cultivates a basic interpersonal skills
  • Course that cultivates an ability for utilizing knowledge
Active-learning course
Most classes are interactive
Course by professor with work experience
Work experience Work experience and relevance to the course content if applicable
N/A N/A
Education related SDGs:the Sustainable Development Goals
  • 4.QUALITY EDUCATION
Last modified : Sat Mar 08 04:19:30 JST 2025