Applied Analytical Chemistry

Course title

D0026000

Course description

Learn the basics of partitioning equilibrium and solvent extraction, photoanalytical methods, electrochemical methods and chromatography.

Purpose of class

To further develop the content of analytical chemistry learned in the first year and to gain an overview of the various analytical methods used in analytical chemistry.

Goals and objectives

Understand distribution equilibria, solvent extraction, and solid-phase extraction
Understand the principles, advantages and disadvantages of photoanalytical methods
Understand the principles, advantages and disadvantages of electrochemical analysis methods
Understand the principles, advantages and disadvantages of chromatography

Relationship between 'Goals and Objectives' and 'Course Outcomes'

	中間試験	期末試験	Total.
1.	25%		25%
2.	25%		25%
3.		25%	25%
4.		25%	25%
Total.	50%	50%	-

Evaluation method and criteria

Achievement Targets 1 and 2 will be evaluated by a mid-term examination that includes the items of the Achievement Targets, and Achievement Targets 3 and 4 will be evaluated by a final examination that includes the items of the Achievement Targets.
The pass/fail grade for a course is calculated as (mid-term exam: 50 points) + (final exam: 50 points), with a total score of 60 points or higher being considered passing.

Language

Japanese

Class schedule

	Class schedule	HW assignments (Including preparation and review of the class.)	Amount of Time Required
1.	Partitioning equilibrium Partition law, partition ratio, partition equilibrium of weak acids, chelate extraction	Read p.166-177 of Analytical Chemistry from the Basics	100minutes
2.	Solvent Extraction Chelating extraction, ion pair extraction, multi-step extraction	Read p.177-189 of Analytical Chemistry from the Basics	100minutes
3.	Solid Phase Extraction What is solid-phase extraction? Solid-liquid equilibrium, ion-exchange equilibrium, other solid-phase extractants, solid-phase extractants and their applications	Read p.190-212 of Analytical Chemistry from the Basics	100minutes
4.	Optical Analysis Method 1 Properties and types of electromagnetic waves, absorption and emission of light, absorption and emission of light from atoms, absorption and emission of light by molecules, Lambert-bert rule	Read p. 56-72 of Instrumental Analytical Chemistry from the Basics	100minutes
5.	Photoanalytical Method 2 Absorption spectrophotometry, Fluorescence spectrophotometry	Read Instrumental Analytical Chemistry from the Basics p.88-111	100minutes
6.	Photoanalytical Method 3 Atomic absorption spectrophotometry, ICP emission spectrometry	Read Instrumental Analytical Chemistry from the Basics p. 73-87	100minutes
7.	Mid-term examination The scope will be 1-6 above. No reference to the textbook or handouts is allowed. After the examination, an explanation of the examination will be given.	Review of mid-term exam coverage	400minutes
8.	Electrochemical Analysis Methods 1 Principles and measurements of potentiometry, potentiometer, indicating electrode, reference electrode, liquid-to-liquid potential, practical examples of potentiometry	Read Instrumental Analytical Chemistry from the Basics p.14-28	100minutes
9.	Electrochemical Analysis Method 2 Practical voltammogram and voltammetry	Read Instrumental Analytical Chemistry from the Basics p. 29-44	100minutes
10.	Electrochemical Analysis Methods 3 Principles and measurements of coulometry, applications of coulometric titration methods	Read Instrumental Analytical Chemistry from the Basics p. 45-55	100minutes
11.	Chromatography 1 Classification and characteristics of chromatography, principles of chromatography and chromatograms	Read Instrumental Analytical Chemistry from the Basics p.166-177	100minutes
12.	Chromatography 2 Principles of gas chromatography, instrumentation features, measurement methods and applications	Read Instrumental Analytical Chemistry from the Basics p.178-193	100minutes
13.	Chromatography 3 Principles of liquid chromatography, instrumentation features, measurement methods and applications	Read Instrumental Analytical Chemistry from the Basics p.194-216	100minutes
14.	Final Examination The scope of the examination will be 7-13 above. No reference to the textbook or handouts is allowed. After the examination, an explanation of the examination will be given.	Review of the scope of the final examination	400minutes
Total.	-	-	2000minutes

Feedback on exams, assignments, etc.

ways of feedback	specific contents about "Other"
Feedback in outside of the class (ScombZ, mail, etc.)

Textbooks and reference materials

1) Analytical Chemistry from the Basics, Hisanori Imura and Teruo Higami, Chemistry Doujin
2) Basic Instrumental Analytical Chemistry, Hisanori Imura and 1 other author, Chemistry Doujin

Reference books: "Basic Chemistry Course: Analytical Chemistry I" by Hisanori Imura, Koji Suzuki, Toshiyuki Homo / Maruzen, "Christian: Analytical Chemistry I, Basic" by Masahiko Tsuchiya, Shozo Toda, Koki Haraguchi / Maruzen, "Analytical Chemistry" by Kosaburo Ohashi and 3 others / Sankyo Publishing, "Textbook Series: Introduction to Analytical Chemistry" by Minoru Tanaka and 2 others / Maruzen, "Basic Chemistry Series 7: Basic Analytical Chemistry" by Koichi Oguma and 5 others / Asakura Shoten, "Quantitative Analytical Chemistry Revised Edition" by Yasuo Torii and Sankyo Yasutomo / Baifukan, "Environmental Analytical Chemistry" by Makoto Aihara and 5 others / Sankyo Publishing, "Analytical Chemistry" by Abe, Shibukawa, Tsunoda / Tokyo Chemical Dojin, "Basic Analytical Chemistry" by Makoto Takagi / Chemical Dojin, and many others

Prerequisites

Studying a subject of Analytical Chemistry, Physical Chemistry 1 and 2

Office hours and How to contact professors for questions