Course title
M20650001
Instrumental Analysis

PAOLO MELE

SAKAI Naomichi

RZEZNICKA IZABELA IRENA

KLIMKOWICZ ALICJA
and more...

SHIBLEE KUMKUM AHMED
Middle-level Diploma Policy (mDP)
Program / Major mDP Goals
先進国際課程 A-1 A-1 Students shall obtain basic and advanced knowledge and skills in mathematics, natural and computer sciences as well as presentation skills to communicate on their knowledge with scholars from various fields.
(改組前)先進国際課程 A-1 A-1 Students shall obtain basic and advanced knowledge and skills in mathematics, natural and computer sciences as well as presentation skills to communicate on their knowledge with scholars from various fields.
Purpose of class
The students will be able to use the standard characterization techniques which constitute the grounds of applied materials science. Students will be able to explain the basic scientific and technical principles of advanced equipment and apply them in the laboratory, to obtain reliable data.They will also obtain experience on how to work in a team, write experimental reports and prepare presentations.
Course description
The theoretical classes (1, 3, 5, 8, 10, 12) and exam classes (7 and 14) are held in the classroom, while the laboratory classes (2, 4, 6, 9, 11, 13) are held in technoplaza common facilities.
In order to become an excellent engineer or researcher, it is mandatory to afford experiments in laboratory and know the theory behind experimental techniques. This course is given by international faculty members. Various experimental techniques are introduced such as: X-Ray Diffraction (XRD); Physical Properties Measurement System (PPMS); Fourier-Transform Infra-Red spectroscopy (FT-IR); Scanning Electron Microscopy (SEM;) Raman spectroscopy;. Thermogravimetry and Differential Thermal Analysis (TG/DTA). For each technique, one class about working principles and introduction to the chemical and/or physical theory behind will be given, followed by a class of basic experience in laboratory. The students will be divided in small groups (3 or 4 each) and each group will team to prepare the reports and presentations of each experience.
Goals and objectives
  1. Students will be able to explain the basic scientific and technical principles of several measuring techniques used in material science.
  2. The students will be able to prepare and deliver public presentations.
  3. The students will be able to conduct basic experiments in the lab, and write scientific reports
Relationship between 'Goals and Objectives' and 'Course Outcomes'

Questionnaire 1 Questionnaire 2 Presentation 1 Presentation 2 6 reports Total.
1. 10% 10% 20%
2. 20% 20% 40%
3. 40% 40%
4. 0%
5. 0%
Total. 10% 10% 20% 20% 40% -
Evaluation method and criteria
Each questionnaire will contribute for 10% to student`s grade. Totally 2 questionnaires will be replied in the classroom so total score for the questionnaires is at maximum 20% of the grade

Each presentation will contribute for 20% to student`s grade. Totally 2 presentations must be provided (for one technique of choice from the first three and for one technique of choice from the second three) so total score for the presentations is at maximum 40% of the grade

Each report will contribute for 6.66% to student`s grade.
Totally 6 reports must be provided (for every experimental class) so total score for the reports is at maximum 40% of the grade

To pass the student must earn a total score of 60% or more.
Language
English
Class schedule

Class schedule HW assignments (Including preparation and review of the class.) Amount of Time Required
1. Introduction to the course - explanation on how prepare reports and presentations;
XRD - theory and principles
lecture review at home 190minutes
2. XRD - laboratory preparation of report 190minutes
3. PPMS - principles of transport measurements lecture review at home 190minutes
4. PPMS -laboratory preparation of report 190minutes
5. FT-IR spectroscopy -theory lecture review at home 190minutes
6. FT-IR spectroscopy - laboratory preparation of report 190minutes
7. First part: questionnaire #1 in class, discussion of reports of the first three laboratories (XRD, PPMS and FT-IR ) and presentation in the class on a technique of choice of the first three preparation of exam #1 185minutes
8. Electron microscopies and SEM - theory lecture review at home 190minutes
9. Electron microscopies and SEM - laboratory preparation of report 190minutes
10. Raman specroscopy - theory lecture review at home 190minutes
11. Raman specroscopy - laboratory preparation of report 190minutes
12. TG/DTA -theory lecture review at home 190minutes
13. TG/DTA - laboratory preparation of report 190minutes
14. Second part: questionnaire #2 in the class, discussion of reports of the second three laboratories (SEM, Raman spectroscopy, and TG/DTA) and presentation in the class on a technique of choice of the second three preparation of exam #2 185minutes
Total. - - 2650minutes
Feedback on exams, assignments, etc.
ways of feedback specific contents about "Other"
Feedback in the class
Textbooks and reference materials
Handouts and manuals distributed in classroom
Prerequisites
Basic Chemistry, Basic Physics
Office hours and How to contact professors for questions
  • Contact via e-mail, the e-mail addresses to the teachers of each class to establish an appointment (substitute ”[at] with ”@”)
  • Introduction and coordination: P. Mele pmele[at]shibaura-it.ac.jp
    XRD: A. Klimkowicz alicja[at]shibaura-it.ac.jp
    PPMS: N. Sakai nsakai[at]shibaura-it.ac.jp
    FT-IR: K. Ahmed kumkum[at]shibaura-it.ac.jp
  • SEM: A. Klimkowicz alicja[at]shibaura-it.ac.jp
    Raman: I. I. Rzeznicka izabela[at]shibaura-it.ac.jp
    TG/DTA: K. Ahmed kumkum[at]shibaura-it.ac.jp
Regionally-oriented
Non-regionally-oriented course
Development of social and professional independence
  • Course that cultivates an ability for utilizing knowledge
  • Course that cultivates a basic problem-solving skills
Active-learning course
About half of the classes are interactive
Course by professor with work experience
Work experience Work experience and relevance to the course content if applicable
N/A N/A
Education related SDGs:the Sustainable Development Goals
  • 7.AFFORDABLE AND CLEAN ENERGY
  • 9.INDUSTRY, INNOVATION AND INFRASTRUCTURE
  • 12.RESPONSIBLE CONSUMPTION & PRODUCTION
Last modified : Sat Mar 14 13:33:25 JST 2026